[1]孟雷,袁其朋.利用大孔树脂从大豆糖蜜中回收大豆异黄酮[J].大豆科学,2007,26(03):435-3438.[doi:10.3969/j.issn.1000-9841.2007.03.031]
　MENG Lei,YUAN Qi-peng.RECOVERY OF ISOFLAVONE FROM SOY MOLASSES BY MACROPOROUS RESIN[J].Soybean Science,2007,26(03):435-3438.[doi:10.3969/j.issn.1000-9841.2007.03.031]
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利用大孔树脂从大豆糖蜜中回收大豆异黄酮

《大豆科学》[ISSN:1000-9841/CN:23-1227/S] 卷: 第26卷 期数: 2007年03期 页码: 435-3438 栏目: 出版日期: 2007-06-25
Title:
RECOVERY OF ISOFLAVONE FROM SOY MOLASSES BY MACROPOROUS RESIN
文章编号:
1000-9841(2007)03-0435-04
作者:
孟雷; 袁其朋
北京化工大学生命科学与技术学院，北京 100029
Author(s):
MENG Lei; YUAN Qi-peng
College of Life Science and Technology,Beijing University of Chemical Technology,Beijing 100029
关键词:
大豆糖蜜; 大豆异黄酮; 大孔树脂; 吸附
Keywords:
Soy molasses; Isoflavone; Macroporous resin; Adsorption
分类号:
TQ655
DOI:
10.3969/j.issn.1000-9841.2007.03.031
文献标志码:
A
摘要:
以大豆糖蜜为原料，以Ca(OH)2为絮凝剂去除大豆蛋白质，利用大孔树脂分离大豆异黄酮。测定了大豆异黄酮在ADS-7型树脂上的吸附饱和曲线，并研究了大豆异黄酮的洗脱条件。结果表明，用浓度为70％的乙醇洗脱大豆异黄酮，得到产品的纯度最高为63.51%，收率为93.40%。
Abstract:
Recovery of isoflavone from soy molasses by macroporous resin was studied.The protein was flocculated from the soy molasses using Ca(OH)2?at room temperature.The break through curve of isoflavone on ADS-7 resin column and the condition of desorption were also investigated.The results showed that the highest purity was obtained when the soy isoflavone was eluted by 70%(V:V) ethanol.The purity and the recovery of the isoflavone were 63.51% and 93.40％,respectively.

参考文献/References:

［1］Tetsu.Akiyama,Junko Ishida.Genistein,a specific inhibitor of tyrosine-specific protein kinases[J].The Journal of Biological Chemistry.1987,262(12):5592-5595.

［2］Shaw Watanabe,Sayo Uesugi,Yuriko Kikuchi.Isoflavones for prevention of cancer,cardiovascular diseases,gynecological problems and possible immune potentiation[J].Biomedicine & Pharmacotherapy.2002,56:302-312.
［3］P.Foti,D.Erba,P.Riso,et al.Comparison between daidzein and genistein antioxidant activity in primary and cancer lymphocytes[J]Archives of Biochemistry and Biophysics.2005,433:421-427.
［4］胡卫新,王晓磊,张洁.大豆异黄酮提取条件和大豆蛋白质分离工艺研究[J].大豆科学,2005,24(1):26-29.
［5］刘国庆,朱翠萍,王占生.大孔树脂对大豆乳清废水中异黄酮的吸附特性研究[J].离子交换与吸附,2003,19(3):229-234.
［6］贾乃堃,袁其朋.高纯度大豆黄苷及大豆黄素的制备[J].大豆科学,2004,23(1):11-14.
［7］于阿娟,谷克仁,冶保献.大豆异黄酮的精制工艺研究[J].中国油脂,2004,29(4):29-31

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备注/Memo

基金项目：企业合作.

作者简介：孟雷（1981－），男，硕士研究生，研究方向制药工程。

更新日期/Last Update: 2014-10-22